Limonin(1180-71-8) ¹³C NMR

Mass

MS2015-05180CW      
limonin
C26H30O8            (Mass of molecular ion:    470)

   Source Temperature: 245 °C
   Sample Temperature:  25 °C
   Direct, 70 eV

      28.0       1.1
      39.0       1.2
      41.0       4.7
      43.0       6.3
      53.0       1.8
      55.0       2.0
      59.0       1.2
      65.0       1.4
      67.0       2.7
      69.0       3.6
      77.0       3.9
      79.0       4.2
      81.0       3.2
      82.0       1.0
      83.0       1.0
      91.0       6.6
      92.0       1.1
      93.0       5.3
      95.0      10.3
      96.0       1.1
      97.0       1.4
     105.0       4.9
     106.0       1.5
     107.0       5.5
     108.0       8.6
     109.0       4.5
     111.0       1.7
     115.0       1.6
     117.0       1.9
     119.0       3.8
     120.0       1.0
     121.0       5.4
     122.0       1.2
     123.0       2.8
     125.0       1.0
     128.0       1.7
     129.0       2.1
     130.0       1.1
     131.0       2.4
     132.0       1.1
     133.0       3.6
     134.0       1.1
     135.0      12.0
     136.0       5.8
     137.0       3.2
     141.0       1.2
     142.0       1.1
     143.0       2.5
     144.0       1.0
     145.0       3.2
     146.0       1.1
     147.0       3.5
     148.0       1.5
     149.0       2.6
     151.0       2.4
     153.0       1.5
     155.0       1.5
     157.0       2.7
     158.0       1.2
     159.0       3.5
     160.0       1.5
     161.0       3.4
     163.0       2.5
     165.0       2.2
     167.0       2.3
     168.0       1.0
     169.0       2.9
     171.0       2.5
     173.0       2.9
     175.0       2.0
     177.0       1.4
     179.0       1.1
     181.0       1.4
     183.0       2.4
     185.0       2.4
     187.0       3.2
     188.0       1.3
     189.0       1.8
     190.0       1.0
     191.0       1.5
     192.0       1.0
     193.0       1.2
     195.0       3.0
     197.0       1.9
     199.0       2.4
     201.0       2.7
     203.0       1.4
     206.0       1.3
     207.0       1.7
     209.0       1.4
     211.0       1.7
     213.0       2.1
     215.0       2.2
     217.0       1.5
     223.0       1.6
     225.0       1.9
     227.0       2.0
     229.0       2.5
     231.0       1.2
     241.0       2.2
     243.0       1.8
     245.0       1.5
     251.0       1.0
     257.0       1.6
     259.0       1.7
     264.0       1.6
     269.0       1.9
     271.0       1.4
     275.0       1.3
     287.0       3.9
     311.0       1.0
     329.0       7.1
     330.0       2.2
     331.0       4.7
     332.0       1.1
     345.0       1.9
     346.0       1.4
     347.0     100.0
     348.0      21.6
     349.0       3.4
     356.0       1.2
     358.0       2.5
     413.0       4.6
     414.0       1.6
     455.0       1.6