3,5-DIBROMOSALICYLAMIDE(17892-25-0) IR2
Product Name3,5-DIBROMOSALICYLAMIDE
CAS17892-25-0
Molecular FormulaC7H5Br2NO2
Molecular Weight294.93
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MassMS-NW-9939 3,5-dibromosalicylamide C7H5Br2NO2 (Mass of molecular ion: 293)
Source Temperature: 160 °C Sample Temperature: 110 °C Direct, 75 eV
17.0 1.8 18.0 10.0 28.0 2.6 37.0 2.0 38.0 1.6 39.0 1.1 44.0 7.8 44.5 1.1 45.0 1.0 50.0 1.5 51.0 1.6 52.0 1.7 53.0 4.2 53.5 4.5 61.0 6.2 62.0 13.2 63.0 10.3 64.0 1.8 74.0 1.7 78.0 1.3 79.0 1.5 80.0 2.3 82.0 2.2 85.0 1.5 86.0 1.1 88.0 1.0 89.0 1.2 90.0 3.3 91.0 3.8 92.0 1.2 107.0 2.6 108.0 2.2 117.0 1.4 119.0 1.3 125.0 1.1 141.0 8.1 142.0 1.7 143.0 8.8 144.0 1.4 147.5 1.1 158.0 1.0 169.0 2.4 170.0 3.8 171.0 2.5 172.0 2.8 197.0 9.3 198.0 2.6 199.0 9.2 200.0 2.0 220.0 3.0 221.0 1.4 222.0 5.9 223.0 2.6 224.0 2.9 225.0 1.2 248.0 5.6 249.0 1.3 250.0 10.6 251.0 1.4 252.0 5.3 275.0 1.0 276.0 51.3 277.0 6.8 278.0 100.0 279.0 10.2 280.0 49.3 281.0 4.6 293.0 21.8 294.0 1.9 295.0 42.4 296.0 3.6 297.0 20.8 298.0 1.7
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7 H5 Br2 N O2 0.035 g : 0.5 ml DMSO-d6 3,5-dibromosalicylamide 
Assign. Shift(ppm)
A 14.3 B *1 8.74 C *1 8.34 D 8.166 E 7.967
Hz ppm Int.5717.12 14.306 1000 3492.24 8.739 179 3334.33 8.344 186 3264.88 8.170 824 3262.74 8.164 890 3185.17 7.970 1000 3182.82 7.965 953 3180.47 7.959 55
in DMSO-d6
KBr disc
nujol mull
