2-Chloro-N,N-diethylacetamide(2315-36-8) 1H NMR
Product Name2-Chloro-N,N-diethylacetamide
CAS2315-36-8
Molecular FormulaC6H12ClNO
Molecular Weight149.62
InChIInChI=1S/C6H12ClNO/c1-3-8(4-2)6(9)5-7/h3-5H2,1-2H3
InChIKey CQQUWTMMFMJEFE-UHFFFAOYSA-N
SmilesC(N(CC)CC)(=O)CCl
-
MassMS-NW-1291 N,N-diethylchloroacetamide C6H12ClNO (Mass of molecular ion: 149)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
14.0 1.2 15.0 5.0 18.0 2.3 26.0 1.8 27.0 13.0 28.0 9.4 29.0 30.8 30.0 14.4 41.0 3.4 42.0 13.7 43.0 3.5 44.0 18.3 49.0 7.3 51.0 2.3 56.0 6.9 57.0 1.7 58.0 100.0 59.0 3.7 70.0 1.3 71.0 1.8 72.0 42.9 73.0 1.7 77.0 6.6 79.0 2.2 86.0 1.2 100.0 20.4 101.0 1.2 106.0 4.8 108.0 1.7 114.0 54.1 115.0 4.1 134.0 12.9 136.0 4.2 149.0 10.8 151.0 3.5
90 MHz in CDCl3
-
1H NMR 89.56 MHz C6 H12 Cl N O 0.04 ml : 0.5 ml CDCl3 N,N-diethylchloroacetamide 
Assign. Shift(ppm)
A 4.070 B *1 3.397 C *1 3.383 D *2 1.241 E *2 1.159
Hz ppm Int.364.50 4.070 1000 315.00 3.518 50 313.88 3.505 53 307.88 3.438 158 306.69 3.425 165 300.81 3.359 169 299.56 3.345 170 293.75 3.280 58 292.38 3.265 60 118.31 1.322 151 111.25 1.243 310 109.88 1.227 205 106.75 1.192 32 103.94 1.161 167 102.69 1.147 317 95.56 1.067 126
in CDCl3
CCl4 solution
liquid film
4880 A,200 M,liquid
