2,6-dichloro-4-mesylaniline (80866-96-2) ¹³C NMR

Mass

MS-IW-0840          
2,6-dichloro-4-mesylaniline
C7H7Cl2NO2S         (Mass of molecular ion:    239)

   Source Temperature: 150 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      15.0       2.1
      18.0       2.1
      28.0       1.6
      36.0       1.3
      39.0       1.1
      52.0       3.9
      61.0       1.7
      62.0       3.9
      63.0       6.5
      64.0       1.0
      65.0       1.7
      73.0       4.0
      74.0       1.1
      75.0       2.6
      76.0       1.3
      78.0       1.1
      88.0       1.9
      89.0       4.2
      90.0       6.9
      97.0       5.8
      98.0       1.7
      99.0       2.6
     112.0       1.1
     124.0      40.9
     125.0       8.2
     126.0      13.7
     127.0       2.7
     133.0       9.6
     134.0       1.0
     135.0       6.2
     137.0       1.0
     140.0       1.5
     148.0       3.8
     150.0       2.4
     159.0       1.5
     160.0      48.4
     161.0       4.9
     162.0      30.9
     163.0       2.6
     164.0       5.3
     176.0      74.2
     177.0       5.4
     178.0      47.7
     179.0       4.7
     180.0       8.0
     181.0       1.9
     196.0       1.0
     208.0       4.1
     210.0       2.9
     224.0      90.4
     225.0       7.1
     226.0      62.1
     227.0       5.0
     228.0      12.1
     229.0       1.0
     239.0     100.0
     240.0       9.3
     241.0      69.0
     242.0       6.3
     243.0      14.1
     244.0       1.3
     245.0       1.2
     258.0       1.1
     260.0       1.1

Assign. Shift(ppm) A 7.760 B 5.07 C 3.046

     Hz     ppm     Int.

   3101.44   7.761    615
   2027.95   5.075     72
   1217.41   3.047   1000