18486-69-6

桃金娘烯醛(18486-69-6)红外图谱(IR1)

产品名称:桃金娘烯醛

CAS:18486-69-6

分子式:C10H14O

分子量: 150.22

Mass

MS-NW-7496          
(1R)-(-)-myrtenal
C10H14O             (Mass of molecular ion:    150)

   Source Temperature: 260 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       1.1
      18.0       1.0
      26.0       1.0
      27.0      19.4
      28.0       2.8
      29.0      10.4
      38.0       2.0
      39.0      27.0
      40.0       4.5
      41.0      35.3
      42.0       2.4
      43.0      16.6
      50.0       4.2
      51.0      12.1
      52.0       5.4
      53.0      17.3
      54.0       2.7
      55.0       9.5
      56.0       1.7
      57.0       1.2
      59.0       3.5
      62.0       1.1
      63.0       3.6
      64.0       1.0
      65.0      10.1
      66.0      14.2
      67.0      12.7
      68.0       4.7
      69.0       4.7
      75.0       1.0
      77.0      35.3
      78.0       8.2
      79.0     100.0
      80.0      11.7
      81.0       8.3
      82.0       2.3
      83.0       2.5
      90.0       1.6
      91.0      32.6
      92.0       7.7
      93.0      13.6
      94.0      12.4
      95.0       6.9
      96.0       2.3
     103.0       2.8
     104.0       1.3
     105.0      24.9
     106.0      32.1
     107.0      67.2
     108.0      37.9
     109.0       7.3
     115.0       2.9
     116.0       1.0
     117.0       8.3
     118.0       1.1
     119.0       2.7
     120.0       1.0
     121.0       7.8
     122.0       3.0
     123.0       1.1
     131.0       1.6
     132.0       1.7
     133.0       1.4
     135.0      14.7
     136.0       1.7
     149.0       1.3
     150.0       2.8

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₁₄ O	0.05 ml : 0.5 ml CDCl₃
(1R)-(-)-myrtenal

    Assign.     Shift(ppm)

      A             9.443
      B             6.726
      C             2.865
      D             2.585
      E             2.560
      F             2.490
      J             2.194
      K     *1      1.341
      L             1.057
      M     *1      0.746

     Hz     ppm     Int.

   3774.17   9.444    458
   2692.99   6.739     55
   2691.53   6.735    103
   2689.82   6.731    135
   2688.23   6.727    192
   2686.77   6.723    145
   2684.94   6.719    108
   2683.59   6.715     62
   1151.73   2.882     70
   1150.27   2.879     77
   1146.00   2.868    130
   1144.65   2.865    142
   1140.38   2.854     77
   1139.04   2.851     83
   1036.25   2.593    101
   1033.08   2.585    182
   1030.03   2.578    109
   1026.12   2.568    126
   1023.19   2.561    200
   1020.26   2.553    132
   1004.88   2.515     79
    999.39   2.501    133
    999.02   2.500    134
    995.61   2.492     76
    993.53   2.486     79
    989.87   2.477    127
    984.25   2.463     73
    884.52   2.214     31
    883.30   2.211     47
    881.96   2.207     50
    880.37   2.203     69
    878.91   2.200     69
    877.44   2.196     86
    875.98   2.192     87
    874.63   2.189     70
    873.17   2.185     66
    871.70   2.182     48
    870.12   2.178     44
    536.13   1.342    949
    528.44   1.323     31
    427.00   1.069    243
    417.85   1.046    239
    298.10   0.746   1000

in CDCl3