2316-64-5

5-溴-2-羟基苯甲醇(2316-64-5)核磁图(¹HNMR)

产品名称:5-溴-2-羟基苯甲醇

CAS:2316-64-5

分子式:C7H7BrO2

分子量: 203.03

InChI:InChI=1S/C7H7BrO2/c8-6-1-2-7(10)5(3-6)4-9/h1-3,9-10H,4H2

InChIKey: KNKRHSVKIORZQB-UHFFFAOYSA-N

Smiles:C1(CO)=CC(Br)=CC=C1O

Mass

MS-IW-0839          
5-bromo-2-hydroxybenzyl alcohol
C7H7BrO2            (Mass of molecular ion:    202)

   Source Temperature: 110 °C
   Sample Temperature:  90 °C
   Direct, 75 eV

      18.0       2.5
      38.0       4.6
      39.0       4.3
      50.0       3.5
      51.0      10.4
      52.0       1.9
      53.0       2.1
      61.5       4.9
      62.0       1.6
      63.0       3.0
      64.0       1.2
      65.0       4.0
      66.0       1.6
      74.0       1.4
      75.0       5.2
      76.0       4.6
      77.0      56.7
      78.0       7.6
      79.0       1.4
      91.0       1.5
      92.0       5.5
      93.0       1.2
      94.0      10.5
      95.0       1.0
     105.0       2.0
     121.0       1.5
     143.0       1.0
     145.0       1.0
     155.0       2.8
     156.0      33.3
     157.0       5.2
     158.0      32.2
     159.0       2.4
     183.0       1.1
     184.0     100.0
     185.0       9.7
     186.0      98.3
     187.0       8.4
     188.0       1.2
     199.0       1.8
     200.0       1.2
     201.0       2.0
     202.0      45.7
     203.0       3.7
     204.0      43.5
     205.0       3.4

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₇ H₇ Br O₂	0.038 g : 0.5 ml DMSO-d₆
5-bromo-2-hydroxybenzyl alcohol

    Assign.     Shift(ppm)

      A             9.7
      B             7.408
      C             7.198
      D             6.734
      E             4.8
      F             4.461

     Hz     ppm     Int.

   3876.50   9.700    124
   2962.04   7.412    304
   2959.44   7.406    317
   2882.54   7.213    182
   2879.94   7.207    171
   2873.99   7.192    199
   2871.40   7.185    189
   2695.47   6.745    459
   2686.92   6.724    429
   1782.99   4.462   1000

in DMSO-d6