5446-18-4

2,4-二氯苯肼盐酸盐(5446-18-4)核磁图(¹³CNMR)

产品名称:2,4-二氯苯肼盐酸盐

CAS:5446-18-4

分子式:C6H7Cl3N2

分子量: 213.49

InChI:InChI=1S/C6H6Cl2N2.ClH/c7-4-1-2-6(10-9)5(8)3-4;/h1-3,10H,9H2;1H

InChIKey: DDWYGJVFURAIJZ-UHFFFAOYSA-N

Smiles:C1(NN)=CC=C(Cl)C=C1Cl.Cl

Mass

MS-IW-8184          
(2,4-dichlorophenyl)hydrazine hydrochloride
C6H6Cl2N2 HCl       (Mass of molecular ion:    176)

   Source Temperature: 160 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      17.0       1.5
      18.0       4.2
      28.0       4.1
      29.0       1.6
      31.0       1.2
      35.0       2.1
      36.0      34.9
      37.0       1.7
      38.0      12.0
      44.5       1.4
      49.0       1.2
      50.0       3.1
      51.0       2.5
      52.0       3.0
      61.0       2.2
      62.0       2.9
      62.5       1.7
      63.0       4.5
      64.0       1.3
      70.0       1.3
      73.0       5.0
      74.0       5.0
      75.0       9.8
      76.0       2.8
      77.0       2.5
      78.0       1.4
      80.5       1.3
      84.0       1.1
      85.0       2.0
      87.0       1.1
      88.0       6.0
      89.0       3.5
      90.0       3.4
      97.0       2.3
      98.0       1.9
      99.0       3.2
     109.0       3.4
     110.0       2.1
     111.0      13.8
     112.0       2.7
     113.0       4.2
     114.0       1.6
     124.0       9.0
     125.0       5.8
     126.0       5.2
     127.0       2.1
     133.0      29.7
     134.0       2.4
     135.0      19.4
     136.0       1.5
     137.0       3.1
     141.0       5.3
     143.0       1.9
     145.0       3.0
     146.0      13.2
     147.0       3.7
     148.0       8.7
     149.0       1.4
     150.0       1.4
     159.0       4.8
     160.0      83.6
     161.0      31.7
     162.0      55.7
     163.0      18.7
     164.0       9.7
     165.0       3.1
     174.0       1.8
     175.0       2.6
     176.0     100.0
     177.0       8.8
     178.0      63.6
     179.0       5.0
     180.0      10.3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₆ Cl₂ N₂	0.034 g : 0.5 ml DMSO-d₆
(2,4-dichlorophenyl)hydrazine hydrochloride

    Assign.     Shift(ppm)

      A            10.6
      B             8.27
      C             7.565
      D             7.418
      E             7.206

     Hz     ppm     Int.

   4219.97  10.560     51
   3305.97   8.273    102
   3024.81   7.569    933
   3022.43   7.563   1000
   2970.78   7.434    413
   2968.40   7.428    375
   2961.99   7.412    499
   2959.60   7.406    474
   2884.14   7.217    749
   2879.38   7.205     35
   2878.83   7.204     35
   2875.35   7.195    643
   2870.77   7.184     26
   2870.40   7.183     24

in DMSO-d6