6315-89-5

3,4-二甲氧基苯胺(6315-89-5)质谱(MS)

产品名称:3,4-二甲氧基苯胺

CAS:6315-89-5

分子式:C8H11NO2

分子量: 153.18

InChI:InChI=1S/C8H11NO2/c1-10-7-4-3-6(9)5-8(7)11-2/h3-5H,9H2,1-2H3

InChIKey: LGDHZCLREKIGKJ-UHFFFAOYSA-N

Smiles:C1(N)=CC=C(OC)C(OC)=C1

Mass

MS-NW-6258          
3,4-dimethoxyaniline
C8H11NO2            (Mass of molecular ion:    153)

   Source Temperature: 240 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       3.3
      18.0       1.5
      26.0       1.0
      27.0       1.6
      28.0       3.6
      29.0       1.1
      33.5       2.8
      38.0       2.0
      39.0       6.2
      40.0       2.5
      41.0      10.3
      42.0       1.6
      50.0       1.9
      51.0       3.9
      52.0       8.1
      53.0       5.0
      54.0       2.2
      55.0       1.3
      61.5       1.3
      62.0       1.1
      63.0       1.6
      64.0       1.0
      65.0       7.9
      66.0       2.6
      67.0      11.4
      68.0       4.5
      69.0       1.7
      77.0       1.0
      78.0       2.9
      79.0       4.3
      80.0       9.3
      81.0       1.6
      82.0       3.1
      92.0       8.1
      93.0       5.2
      94.0       2.1
      95.0      16.5
      96.0       1.3
     107.0       2.4
     108.0       5.7
     109.0       2.6
     110.0      40.1
     111.0       3.0
     122.0       1.6
     125.0       3.0
     137.0       2.6
     138.0      88.5
     139.0       7.7
     152.0       3.2
     153.0     100.0
     154.0       9.2
     155.0       1.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₁₁ N O₂	0.040 g : 0.5 ml CDCl₃
3,4-dimethoxyaniline

    Assign.     Shift(ppm)

      A             6.697
      B             6.299
      C             6.222
      D     *1      3.812
      E     *1      3.794
      F             3.4

     Hz     ppm     Int.

   2680.79   6.708    155
   2672.36   6.687    168
   2519.04   6.304    146
   2516.48   6.297    164
   2491.82   6.236    113
   2489.26   6.229     93
   2483.40   6.214    102
   2480.83   6.208     87
   1523.80   3.813    999
   1516.36   3.795   1000
   1365.84   3.418     22

in CDCl3