67330-62-5

3-氯-2,6-二乙基苯胺(67330-62-5)质谱(MS)

产品名称:3-氯-2,6-二乙基苯胺

CAS:67330-62-5

分子式:C10H14ClN

分子量: 183.68

InChI:InChI=1S/C10H14ClN/c1-3-7-5-6-9(11)8(4-2)10(7)12/h5-6H,3-4,12H2,1-2H3

InChIKey: VDJBIPLKIGSVRG-UHFFFAOYSA-N

Smiles:C1(N)=C(CC)C=CC(Cl)=C1CC

Mass

MS-IW-1780          
3-chloro-2,6-diethylaniline
C10H14ClN           (Mass of molecular ion:    183)

   Source Temperature: 240 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      27.0       1.3
      28.0       1.1
      39.0       2.5
      41.0       1.1
      51.0       3.3
      52.0       1.7
      53.0       1.3
      58.5       1.9
      63.0       2.1
      64.5       1.8
      65.0       3.7
      65.5       1.7
      66.0       1.0
      75.0       1.4
      76.5       6.2
      77.0       5.5
      77.5       2.0
      78.0       1.6
      83.5       1.0
      89.0       1.9
      90.0       1.1
      91.0       5.2
     102.0       1.5
     103.0       2.2
     104.0       1.7
     105.0       1.9
     115.0       4.1
     116.0       2.7
     117.0       6.6
     118.0       3.6
     119.0       2.7
     120.0       1.0
     127.0       1.3
     128.0       1.9
     129.0       1.0
     130.0       3.8
     131.0       3.4
     132.0       4.9
     133.0      10.6
     134.0       1.1
     140.0       1.5
     148.0       2.6
     151.0       1.4
     152.0       1.6
     153.0       5.6
     154.0       2.8
     155.0       2.0
     166.0       1.9
     168.0     100.0
     169.0      10.5
     170.0      31.8
     171.0       3.3
     182.0       2.2
     183.0      39.8
     184.0       5.3
     185.0      13.0
     186.0       1.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₁₄ Cl N	0.05 ml : 0.5 ml CDCl₃
3-chloro-2,6-diethylaniline

    Assign.     Shift(ppm)

      A             6.816
      B             6.752
      C             3.68
      D             2.705
      E             2.425
      F             1.203
      G             1.142

     Hz     ppm     Int.

   2729.25   6.830    184
   2721.07   6.809    312
   2701.42   6.760    363
   2693.24   6.739    216
   1474.37   3.690     55
   1092.53   2.734    146
   1084.84   2.715    418
   1077.27   2.696    423
   1069.70   2.677    152
    980.59   2.454    116
    973.14   2.435    326
    965.58   2.417    332
    957.89   2.397    124
    488.16   1.222    605
    485.84   1.216     34
    480.59   1.203   1000
    478.27   1.197     61
    473.02   1.184    568
    470.83   1.179     39
    464.11   1.162    533
    456.54   1.143    941
    448.85   1.124    513

in CDCl3