78056-67-4

1-benzylpiperidine-4-acetonitrile(78056-67-4)核磁图(¹HNMR)

产品名称:1-benzylpiperidine-4-acetonitrile

CAS:78056-67-4

分子式:C14H18N2

分子量: 214.31

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-8579          
(1-benzyl-4-piperidyl)acetonitrile
C14H18N2            (Mass of molecular ion:    214)

   Source Temperature: 260 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      18.0       1.7
      27.0       2.1
      28.0       2.8
      29.0       1.9
      30.0       1.4
      39.0       4.4
      41.0       5.7
      42.0       8.4
      44.0       3.5
      51.0       2.0
      53.0       1.7
      54.0       1.7
      55.0       3.7
      56.0       1.9
      63.0       1.7
      65.0      12.2
      66.0       1.0
      67.0       2.1
      68.0       1.2
      69.0       1.0
      77.0       1.5
      82.0       6.0
      89.0       2.2
      90.0       1.5
      91.0     100.0
      92.0      20.4
      93.0       1.4
      94.0       1.2
      95.0       1.4
      96.0       4.1
     104.0       1.6
     106.0       1.1
     118.0       2.4
     119.0       1.2
     120.0       4.6
     123.0      35.9
     124.0       3.1
     132.0       2.5
     137.0      31.1
     138.0       2.9
     146.0       3.4
     170.0       1.2
     172.0       2.3
     174.0       7.9
     175.0       1.1
     213.0      22.5
     214.0      21.3
     215.0       3.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₈ N₂	0.05 ml : 0.5 ml CDCl₃
(1-benzyl-4-piperidyl)acetonitrile

    Assign.     Shift(ppm)

      A             7.29
      B             7.233
      C             3.470
      D             2.870
      E             2.224
      F             1.952
      G             1.736
      J             1.632
      K             1.375

     Hz     ppm     Int.

   2924.56   7.318     31
   2923.46   7.316     33
   2921.75   7.311     36
   2918.09   7.302     82
   2915.77   7.296    596
   2911.25   7.285   1000
   2907.10   7.275     75
   2904.05   7.267     39
   2902.59   7.263     36
   2899.66   7.256     44
   2895.63   7.246     98
   2892.94   7.239    114
   2892.33   7.238    105
   2890.99   7.234    111
   2886.84   7.224    112
   2884.16   7.217     48
   2882.20   7.212     66
   1386.96   3.471    766
   1154.91   2.890     77
   1152.59   2.884    125
   1149.90   2.878     85
   1143.43   2.862     89
   1140.75   2.855    131
   1137.21   2.846     69
    892.33   2.233    453
    885.62   2.216    479
    781.49   1.956    161
    778.93   1.950    167

in CDCl3