1,5-DIIODO-9,10-ANTHRACENEDIONE synthesis
- Product Name:1,5-DIIODO-9,10-ANTHRACENEDIONE
- CAS Number:3311-73-7
- Molecular formula:C14H6I2O2
- Molecular Weight:460.01
129-44-2
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Yield: 90%
Reaction Conditions:
Stage #1:1,5-diaminoanthraquinone with sulfuric acid;sodium nitrite in water at -20; for 0.5 h;
Stage #2: with potassium iodide in water at -20 - 80; for 5 h;
References:
Iseki, Shuta;Kishida, Sakura;Nonomura, Kohei;Ogata, Daiji;Yuasa, Junpei [Journal of the American Chemical Society,2020,vol. 142,# 37,p. 15842 - 15851] Location in patent:supporting information