1-Adamantanamine hydrochloride synthesis
- Product Name:1-Adamantanamine hydrochloride
- CAS Number:665-66-7
- Molecular formula:C10H18ClN
- Molecular Weight:187.71
768-94-5
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665-66-7
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Yield:665-66-7 100%
Reaction Conditions:
with hydroxylamine hydrochloride in ethanol; for 2 h;Reflux;
Steps:
General procedure for the preparation of amine hydrochloride salts 2c-2r
General procedure: To a 25-mL round-bottomed flask containing ammonium chloride (0.54 g, 10 mmol) was added ethanol (3 mL) followed by the requisite amine (10 mmol). The mixture was magnetically stirred and refluxed for 2 h. The solvent was then removed by rotary evaporation affording the hydrochloride salt as a solid invariably in quantitative yield.
References:
Di Grandi, Martin J.;Bennett, Caitlin;Cagino, Kristen;Muccini, Arnold;Suraci, Corey;Saba, Shahrokh [Synthetic Communications,2015,vol. 45,# 22,p. 2601 - 2607] Location in patent:supporting information
880-52-4
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665-66-7
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7575-82-8
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665-66-7
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3405-48-9
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665-66-7
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281-23-2
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665-66-7
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$16.00/5g