1-FLUORO-3-PHENYLPROPAN-2-AMINE synthesis
- Product Name:1-FLUORO-3-PHENYLPROPAN-2-AMINE
- CAS Number:70824-86-1
- Molecular formula:C9H12FN
- Molecular Weight:153.2
336783-89-2
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70824-86-1
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Yield:-
Reaction Conditions:
with hydrogen;palladium 10% on activated carbon in methanol; under 2280.15 Torr; for 2 h;
Steps:
6
To a solution of (2-azido-3-fluoro-propyl)benzene (0.6 g) in MeOH (50 mL) was added 10% Pd/C catalyst and the suspension was hydrogenated for 2 hr. at 3 atmospheres pressure. The filtered reaction mixture and MeOH washings were concentrated to an oil which was chromatographed over silica gel with an ammoniated mixture of MeOH/ether (1:9) to give 0.38 g of the title compound. MS ES (M++H)=154.
References:
US2005/245595,2005,A1 Location in patent:Page/Page column 10
503-20-8
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$40.30/1g
6921-34-2
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$83.80/50ml
70824-86-1
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