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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List ETHYL 3-(3-CHLORO-2,4,5-TRIFLUOROPHENYL)-3-OXOPROPANOATE
101987-86-4

ETHYL 3-(3-CHLORO-2,4,5-TRIFLUOROPHENYL)-3-OXOPROPANOATE synthesis

3synthesis methods
3-Chloro-2,4,5-trifluorobenzoic acid

101513-77-3
255 suppliers
$20.40/1g

ETHYL 3-(3-CHLORO-2,4,5-TRIFLUOROPHENYL)-3-OXOPROPANOATE

101987-86-4
150 suppliers
$6.00/1g

-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: thionyl chloride / N,N-dimethyl-formamide / 4 h / Reflux
2.1: magnesium / tetrachloromethane; ethanol / 3.25 h / Reflux
2.2: 2.33 h / -10 °C
3.1: toluene-4-sulfonic acid / water / 5 h / Reflux

References:

Huang, Ju;Wang, Minghua;Wang, Bin;Wu, Zhaoyang;Liu, Mingliang;Feng, Lianshun;Zhang, Jun;Li, Xiaoning;Yang, Yang;Lu, Yu [Bioorganic and Medicinal Chemistry Letters,2016,vol. 26,# 9,p. 2262 - 2267]

3-CHLORO-2,4,5-TRIFLUOROBENZOYL CHLORIDE

101513-78-4
57 suppliers
$31.81/1gm:

ETHYL 3-(3-CHLORO-2,4,5-TRIFLUOROPHENYL)-3-OXOPROPANOATE

101987-86-4
150 suppliers
$6.00/1g

References
6148-64-7 Synthesis
Ethyl potassium malonate

6148-64-7
408 suppliers
$5.00/10g

3-CHLORO-2,4,5-TRIFLUOROBENZOYL CHLORIDE

101513-78-4
57 suppliers
$31.81/1gm:

ETHYL 3-(3-CHLORO-2,4,5-TRIFLUOROPHENYL)-3-OXOPROPANOATE

101987-86-4
150 suppliers
$6.00/1g

References

ETHYL 3-(3-CHLORO-2,4,5-TRIFLUOROPHENYL)-3-OXOPROPANOATE Related Search:

Ethyl 2,4,5-trifluorobenzoylacetate 3-Quinolinecarboxylic acid, 8-chloro-6,7-difluoro-1-[(1R,2S)-2-fluorocyclopropyl]-1,4-dihydro-4-oxo- Diphenyl phosphate 3-AMINO-2,4,5-TRIFLUOROBENZOIC ACID