Welcome to chemicalbook!
Chinese English Japanese Germany Korea
010-86108875
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

1068437-26-2

tert-Butyl 7-broMo-2-oxoquinoline-1(2H)-carboxylate synthesis

1synthesis methods
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
796 suppliers
$13.50/25G

99465-10-8 Synthesis
7-Bromoquinolin-2(1H)-one

99465-10-8
112 suppliers
$22.00/100mg

tert-Butyl 7-broMo-2-oxoquinoline-1(2H)-carboxylate

1068437-26-2
1 suppliers
inquiry

-

Yield:1068437-26-2 84%

Reaction Conditions:

Stage #1: 7-bromo-1,2-dihydroquinolin-2-onewith sodium hydride in tetrahydrofuran;mineral oil at 50; for 1 h;
Stage #2: di-tert-butyl dicarbonate in tetrahydrofuran;mineral oil at 50; for 2 h;

References:

Broch, Sidonie;Anizon, Fabrice;Moreau, Pascale [Synthesis,2008,# 13,p. 2039 - 2044] Location in patent:experimental part