Methyl 7-chloro-3-methylbenzo[b]thiophene-2-carboxylate synthesis
- Product Name:Methyl 7-chloro-3-methylbenzo[b]thiophene-2-carboxylate
- CAS Number:1415968-75-0
- Molecular formula:C11H9ClO2S
- Molecular Weight:240.71
2365-48-2
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Yield:1415968-75-0 1.61 g
Reaction Conditions:
with 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene at 0 - 20; for 18 h;Inert atmosphere;
References:
Friberg, Anders;Vigil, Dominico;Zhao, Bin;Daniels, R. Nathan;Burke, Jason P.;Garcia-Barrantes, Pedro M.;Camper, Demarco;Chauder, Brian A.;Lee, Taekyu;Olejniczak, Edward T.;Fesik, Stephen W. [Journal of Medicinal Chemistry,2013,vol. 56,# 1,p. 15 - 30] Location in patent:supporting information