Welcome to chemicalbook!
Chinese English Japanese Germany Korea
010-86108875
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

18054-10-9

Benzoic acid, 4,4'-(1,1,3,3-tetramethyl-1,3-disiloxanediyl)bis- synthesis

10synthesis methods
18055-70-4 Synthesis
1,3-Di(p-tolyl)-1,1,3,3-tetramethyldisiloxane, 97%

18055-70-4
14 suppliers
$65.90/1g

Benzoic acid, 4,4'-(1,1,3,3-tetramethyl-1,3-disiloxanediyl)bis-

18054-10-9
0 suppliers
inquiry

-

Yield:18054-10-9 90%

Reaction Conditions:

Stage #1: 1,3-bis(4′-tolyl)-1,1,3,3-tetramethyldisiloxanewith 1-hydroxy-pyrrolidine-2,5-dione;oxygen;cobalt(II) diacetate tetrahydrate in acetonitrile at 60; under 760.051 Torr; for 24 h;Green chemistry;
Stage #2: with sodium hydrogencarbonate in ethanol;water at 50; for 2 h;Green chemistry;Temperature;

References:

Goncharova, Irina K.;Silaeva, Kseniia P.;Arzumanyan, Ashot V.;Anisimov, Anton A.;Milenin, Sergey A.;Novikov, Roman A.;Solyev, Pavel N.;Tkachev, Yaroslav V.;Volodin, Alexander D.;Korlyukov, Alexander A.;Muzafarov, Aziz M. [Journal of the American Chemical Society,2019,vol. 141,# 5,p. 2143 - 2151] Location in patent:supporting information