(3aR,4R,6aS)-3a,6a-Dihydro-2,2-diemthyl-4H-cyclopenta-1,3-dioxol-4-ol synthesis

6synthesis methods

Product Name:(3aR,4R,6aS)-3a,6a-Dihydro-2,2-diemthyl-4H-cyclopenta-1,3-dioxol-4-ol
CAS Number:185622-62-2
Molecular formula:C8H12O3
Molecular Weight:156.1791

25581-41-3 Synthesis

25581-41-3
108 suppliers
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(3aR,4R,6aS)-3a,6a-Dihydro-2,2-diemthyl-4H-cyclopenta-1,3-dioxol-4-ol

185622-62-2
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 81 percent / diisobutylaluminum hydride / toluene / 1.5 h / -78 - 20 °C
2: 75 percent / NaH; DMSO / tetrahydrofuran / 20 °C
3: oxalyl chloride; DMSO; Et₃N / CH₂Cl₂ / -78 - 20 °C
4: 167 mg / tetrahydrofuran / 1 h / -78 °C
5: 25.7 percent / Grubbs catalyst / CHCl₃ / 4 h / 20 °C

References:

Won Jun Choi;Jae Gyu Park;Su Jeong Yoo;Hea Ok Kim;Hyung Ryong Moon;Moon Woo Chun;Young Hoon Jung;Lak Shin Jeong [Journal of Organic Chemistry,2001,vol. 66,# 19,p. 6490 - 6494]

(+)-(3aS,6aS)-3a,6a-Dihydro-2,2-dimethyl-4H-cyclopenta-1,3-dioxol-4-one

104010-72-2
56 suppliers
$65.00/50mg

185622-62-2
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References

1,3-Dioxolane-4-methanol, α,5-diethenyl-2,2-dimethyl-, (4R,5S)-

369647-26-7
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185622-62-2
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4H-Cyclopenta-1,3-dioxol-4-ol, 3a,6a-dihydro-2,2-dimethyl-, (3aR,4S,6aS)-

369647-29-0
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References

189996-60-9 Synthesis

Furo[3,4-d]-1,3-dioxol-4-ol, tetrahydro-2,2-dimethyl-, (3aR,6aR)-

189996-60-9
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185622-62-2
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References

(4R,5S)-(2,2-Dimethyl-5-vinyl-1,3-dioxolan-4-yl)methan-1-ol

127758-25-2
7 suppliers
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185622-62-2
14 suppliers
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References

(3aR,4R,6aS)-3a,6a-Dihydro-2,2-diemthyl-4H-cyclopenta-1,3-dioxol-4-ol Related Search:

(-)-(3aR,6aR)-3a,6a-Dihydro-2,2-dimethyl-4H-cyclopenta-1,3-dioxol-4-one 4H-Cyclopenta-1,3-dioxol-4-ol, 3a,6a-dihydro-2,2-dimethyl-, (3aS,4S,6aR)-

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