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ChemicalBook CAS DataBase List 2,2,3,3,3-PENTAFLUOROPROPYLAMINE HYDROCHLORIDE
374-14-1

2,2,3,3,3-PENTAFLUOROPROPYLAMINE HYDROCHLORIDE synthesis

2synthesis methods
-

Yield:-

Reaction Conditions:

Stage #1:pentafluoropropionic acid;benzylamine with tetrachloromethane;TEA;triphenylphosphine in chloroform at 80; for 0.666667 h;
Stage #2: with TEA;water at 80; for 12 h;
Stage #3: with hydrogenchloride in methanol for 12 h;Heating;

References:

Soloshonok, Vadim A;Ohkura, Hironari;Uneyama, Kenji [Tetrahedron Letters,2002,vol. 43,# 31,p. 5449 - 5452]