
2,2,3,3,3-PENTAFLUOROPROPYLAMINE HYDROCHLORIDE synthesis
- Product Name:2,2,3,3,3-PENTAFLUOROPROPYLAMINE HYDROCHLORIDE
- CAS Number:374-14-1
- Molecular formula:C3H5ClF5N
- Molecular Weight:185.52
Yield:-
Reaction Conditions:
Stage #1:pentafluoropropionic acid;benzylamine with tetrachloromethane;TEA;triphenylphosphine in chloroform at 80; for 0.666667 h;
Stage #2: with TEA;water at 80; for 12 h;
Stage #3: with hydrogenchloride in methanol for 12 h;Heating;
References:
Soloshonok, Vadim A;Ohkura, Hironari;Uneyama, Kenji [Tetrahedron Letters,2002,vol. 43,# 31,p. 5449 - 5452]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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374-14-1
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