Welcome to chemicalbook!
Chinese English Japanese Germany Korea
010-86108875
logo
Inquriy
Try our best to find the right business for you.
Messages
Do not miss inquiry messages Please log in to view all inquiry messages.
My chemicalbook

Welcome back!

Structured search
18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 2,3,4,5,6-PENTAFLUOROPHENYLACETONITRILE
653-30-5

2,3,4,5,6-PENTAFLUOROPHENYLACETONITRILE synthesis

13synthesis methods
Ethylcyano(pentafluorophenyl)acetate

2340-87-6
6 suppliers
inquiry

2,3,4,5,6-PENTAFLUOROPHENYLACETONITRILE

653-30-5
131 suppliers
$14.00/1g

-

Yield: 97%

Reaction Conditions:

with sulfuric acid;acetic acid in water at 20; for 16.5 h;Reflux;

Steps:

2.2
Step2: Add in the reactorIntermediate A-2-1 (2.79 g, 10 mmol),50% acetic acid (4.10 mL) and sulfuric acid (0.2 mL),Stir after 16 hours of reflux,After the mixture is cooled to room temperature,The reaction was terminated by dropwise addition of 10 mL of cold distilled water.After stirring for 0.5 h,The reaction mixture was extracted with distilled water and chloroform.It was then concentrated to give intermediate A-2-2 (1.95 g, 97%).

References:

Changchun Hai Purunsi Technology Co., Ltd.;Dong Xiuqin;Cai Hui CN109134311, 2019, A Location in patent:Paragraph 0090; 0091; 0093

α-Bromo-2,3,4,5,6-pentafluorotoluene

1765-40-8
201 suppliers
$10.00/1 g

2,3,4,5,6-PENTAFLUOROPHENYLACETONITRILE

653-30-5
131 suppliers
$14.00/1g

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
0 suppliers
inquiry

References
143-33-9 Synthesis
Sodium cyanide

143-33-9
0 suppliers
$10.00/1g

α-Bromo-2,3,4,5,6-pentafluorotoluene

1765-40-8
201 suppliers
$10.00/1 g

2,3,4,5,6-PENTAFLUOROPHENYLACETONITRILE

653-30-5
131 suppliers
$14.00/1g

References
392-56-3 Synthesis
hexafluorobenzene

392-56-3
300 suppliers
$9.00/1g

2,3,4,5,6-PENTAFLUOROPHENYLACETONITRILE

653-30-5
131 suppliers
$14.00/1g

References
POTASSIUM CYANIDE

151-50-8
0 suppliers
$36.40/100g

α-Bromo-2,3,4,5,6-pentafluorotoluene

1765-40-8
201 suppliers
$10.00/1 g

2,3,4,5,6-PENTAFLUOROPHENYLACETONITRILE

653-30-5
131 suppliers
$14.00/1g

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
0 suppliers
inquiry

References

2,3,4,5,6-PENTAFLUOROPHENYLACETONITRILE Related Search:

METHYL PENTAFLUOROPHENYL CARBONATE 2,3,4,5,6-PENTAFLUOROPHENYL 4-NITROBENZENESULFONATE Pentafluorobenzoyl chloride PENTAFLUOROBENZENESULFONYL CHLORIDE Pentafluorobenzyl chloride IODOPENTAFLUOROBENZENE 2,3,4,5,6-Pentafluorobenzyl alcohol 2,3,4,5,6-Pentafluoroaniline Pentafluorobenzonitrile Pentafluorobenzaldehyde