2,3-DICHLOROPYRIDINE-5-BORONIC ACID PINACOL ESTER synthesis
1synthesis methods
- Product Name:2,3-DICHLOROPYRIDINE-5-BORONIC ACID PINACOL ESTER
- CAS Number:741709-64-8
- Molecular formula:C11H14BCl2NO2
- Molecular Weight:273.95
Yield:741709-64-8 44%
Reaction Conditions:
with (1,5-cyclooctadiene)(methoxy)iridium(I) dimer;4,4'-di-tert-butyl-2,2'-bipyridine in tert-butyl methyl ether at 20; for 5 h;Glovebox;Sealed tube;Inert atmosphere;regioselective reaction;
References:
Sadler, Scott A.;Tajuddin, Hazmi;Mkhalid, Ibraheem A. I.;Batsanov, Andrei S.;Albesa-Jove, David;Cheung, Man Sing;Maxwell, Aoife C.;Shukla, Lena;Roberts, Bryan;Blakemore, David C.;Lin, Zhenyang;Marder, Todd B.;Steel, Patrick G. [Organic and Biomolecular Chemistry,2014,vol. 12,# 37,p. 7318 - 7327] Location in patent:supporting information