2,3-Difluoro-6-methoxyphenylboronic acid synthesis
- Product Name:2,3-Difluoro-6-methoxyphenylboronic acid
- CAS Number:957061-21-1
- Molecular formula:C7H7BF2O3
- Molecular Weight:187.94
957061-21-1
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Yield:-
Reaction Conditions:
Stage #1: (2,3-difluoro-6-methoxyphenyl)boronic acidwith boron tribromide in dichloromethane at -78 - 20;Inert atmosphere;
Stage #2: with methanol in dichloromethane at -78;Inert atmosphere;
References:
Vishnumurthy, Kodumuru;Makriyannis, Alexandros [Journal of Combinatorial Chemistry,2010,vol. 12,# 5,p. 664 - 669] Location in patent:experimental part