2-Amino-6-chlorobenzaldehyde synthesis
- Product Name:2-Amino-6-chlorobenzaldehyde
- CAS Number:35490-90-5
- Molecular formula:C7H6ClNO
- Molecular Weight:155.58
39885-08-0
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$6.00/100mg
35490-90-5
57 suppliers
$21.00/100mg
Yield:35490-90-5 96%
Reaction Conditions:
with manganese(IV) oxide in diethyl ether; for 0.5 h;
Steps:
10
To prepare this compound, manganese dioxide (13.6 g, 157 mmol) was added to a solution of 2-(amino-6-chlorophenyl)methanol (2.75 g, 17.5 mmol) in 150 mL diethyl ether. The mixture was stirred for 0.5 hours then filtered through celite and rinsed with ethyl acetate. The filtrate was concentrated under reduced pressure to afford 2.62 g(96%) of 2-amino-6-chlorobenzaldehyde.
References:
WO2006/10142,2006,A2 Location in patent:Page/Page column 70; 71
6361-22-4
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$17.00/250mg
35490-90-5
57 suppliers
$21.00/100mg
387-45-1
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$9.00/1g
35490-90-5
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$21.00/100mg
2148-56-3
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$5.00/10g
35490-90-5
57 suppliers
$21.00/100mg
6575-11-7
135 suppliers
$8.00/1g
35490-90-5
57 suppliers
$21.00/100mg