ChemicalBook CAS DataBase List 1,3-Benzodioxole-5-methanamine, .alpha.-methyl-, (.alpha.R)-

1,3-Benzodioxole-5-methanamine, .alpha.-methyl-, (.alpha.R)- synthesis

1synthesis methods

Product Name:1,3-Benzodioxole-5-methanamine, .alpha.-methyl-, (.alpha.R)-
CAS Number:210488-54-3
Molecular formula:C9H11NO2
Molecular Weight:165.19

3162-29-6 Synthesis

3162-29-6
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1,3-Benzodioxole-5-methanamine, .alpha.-methyl-, (.alpha.R)-

210488-54-3
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: titanium(IV) tetraethanolate / tetrahydrofuran / 30 h / 20 °C / Reflux
2: sodium tetrahydroborate / tetrahydrofuran / 1 h / 0 - 20 °C
3: hydrogenchloride / methanol / 1.25 h / 0 - 20 °C

References:

WO2016/30443,2016,A1

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