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ChemicalBook CAS DataBase List 3-Decylpyridine
59652-33-4

3-Decylpyridine synthesis

3synthesis methods
-

Yield:59652-33-4 67.7%

Reaction Conditions:

Stage #1: 1-bromo dodecanewith magnesium in tetrahydrofuran;Heating;
Stage #2: 3-Bromopyridine;1,2-bis(diphenylphosphino)ethane nickel(II) chloride in tetrahydrofuran;Heating;Further stages.;

References:

Getmanenko, Yulia A.;Twieg, Robert J. [Journal of Organic Chemistry,2008,vol. 73,# 3,p. 830 - 839]

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