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148761-50-6

3-methyl-1lambda6-thiomorpholine-1,1-dione synthesis

2synthesis methods
3-methyl-1lambda6-thiomorpholine-1,1-dione

148761-50-6
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Yield:148761-50-6 86%

Reaction Conditions:

with 3-chloro-benzenecarboperoxoic acid in dichloromethane;1) 0 deg C to room temp., 2) room temp., 1 h;

References:

Gallego, Maria Teresa;Brunet, Ernesto;Ruano, Jose Luis Garcia [Journal of Organic Chemistry,1993,vol. 58,# 15,p. 3905 - 3911]