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32916-63-5

Cyclopropanemethanol, 2,2-dimethyl-3-(2-methyl-1-propen-1-ylidene)- synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: hydrogenchloride; copper; ammonium chloride; copper(l) chloride / water / 3 h / 0 °C
2: dibenzo-18-crown-6; potassium hydroxide / water; benzene / 168 h / 20 °C / Inert atmosphere

References:

Lu, Bei-Li;Shi, Min [Angewandte Chemie - International Edition,2011,vol. 50,# 50,p. 12027 - 12031]