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ChemicalBook CAS DataBase List 3',6'-bis(diethylamino)-2-phenylspiro[1H-isoindole-1,9'-[9H]xanthene]-3(2H)-one
38660-35-4

3',6'-bis(diethylamino)-2-phenylspiro[1H-isoindole-1,9'-[9H]xanthene]-3(2H)-one synthesis

3synthesis methods
-

Yield:38660-35-4 77%

Reaction Conditions:

Stage #1: rhodamine Bwith O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate;triethylamine in 1,2-dichloro-ethane at 20; for 2 h;
Stage #2: aniline in 1,2-dichloro-ethane at 20;

References:

He, Jiaxin;Yan, Boyu;Meng, Jiangtao;Ran, Maogang;Zhou, Yutong;Deng, Jinfei;Li, Chao-Jun;Yao, Qiuli [European Journal of Organic Chemistry,2021,vol. 2021,# 29,p. 4059 - 4064] Location in patent:supporting information

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