(4-propoxyphenyl)methanol synthesis
- Product Name:(4-propoxyphenyl)methanol
- CAS Number:90925-43-2
- Molecular formula:C10H14O2
- Molecular Weight:166.22
5736-85-6
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Yield:90925-43-2 87%
Reaction Conditions:
with methanol;sodium tetrahydroborate at 20; for 1 h;Inert atmosphere;
Steps:
Synthetic procedure 2: reduction of the aldehyde
General procedure: NaBH4 (1.1 mmol) was added to the alkoxy benzyl aldehyde (1.0 mmol) in methanol (5.0 mL) under nitrogen atmosphere. The reaction was stirred for 1 h at room temperature. The reaction mixture was concentrated under reduced pressure and water (20 mL) was added. The mixture was extracted with ethyl acetate (3×20 mL). The combined organic layers were dried with MgSO4, filtered and the solvent was evaporated under reduced pressure.
References:
Eleftheriadis, Nikolaos;Thee, Stephanie;Te Biesebeek, Johan;Van Der Wouden, Petra;Baas, Bert-Jan;Dekker, Frank J. [European Journal of Medicinal Chemistry,2015,vol. 94,p. 265 - 275]
100256-94-8
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60758-84-1
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623-05-2
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106-94-5
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90925-43-2
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40663-68-1
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90925-43-2
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