Welcome to chemicalbook!
Chinese English Japanese Germany Korea
010-86108875
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 2,3,4,6-Tetra-O-acetyl-beta-D-galactopyranosyl cyanide
52443-07-9

2,3,4,6-Tetra-O-acetyl-beta-D-galactopyranosyl cyanide synthesis

6synthesis methods
-

Yield:52443-07-9 79%

Reaction Conditions:

Stage #1: D-Galactose;acetic anhydridewith pyridine;sodium acetate at 100; for 2 h;
Stage #2: trimethylsilyl cyanidewith boron trifluoride diethyl etherate in nitromethane at 35; for 2 h;

References:

Lichtenthaler, Frieder W.;Klotz, Juergen;Nakamura, Katsumi [Tetrahedron Asymmetry,2003,vol. 14,# 24,p. 3973 - 3986]