ChemicalBook CAS DataBase List 4-Methyl-2-phenyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole

4-Methyl-2-phenyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole synthesis

1synthesis methods

Product Name:4-Methyl-2-phenyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole
CAS Number:690632-24-7
Molecular formula:C16H20BNO2S
Molecular Weight:301.21

4-Methyl-2-phenyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole

690632-24-7
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4-Methyl-2-phenyl-5-(trifluoromethyl)thiazole

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: potassium hydrogen bifluoride / methanol; water / 1 h / 20 °C
2: copper(l) chloride; tert.-butylhydroperoxide / methanol; water; dichloromethane / 12 h / 0 - 20 °C

References:

Presset, Marc;Oehlrich, Daniel;Rombouts, Frederik;Molander, Gary A. [Journal of Organic Chemistry,2013,vol. 78,# 24,p. 12837 - 12843]

4-Methyl-2-phenyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole Related Search:

2,4-Dimethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole 2-phenyl-5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-Thiazole

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