5,11-bisthio-(R,R)-1,7-diazatricyclo[7.3.0.07,11]dodecane-2,8-diketone synthesis
- Product Name:5,11-bisthio-(R,R)-1,7-diazatricyclo[7.3.0.07,11]dodecane-2,8-diketone
- CAS Number:72744-67-3
- Molecular formula:C8H10N2O2S2
- Molecular Weight:230.31
67089-84-3
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72744-67-3
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Yield:72744-67-3 70%
Reaction Conditions:
Stage #1: (R)-thiazolidine-4-carboxylic acid hydrochloridewith O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate in acetonitrile at 20; for 0.166667 h;Inert atmosphere;
Stage #2: with N-ethyl-N,N-diisopropylamine in acetonitrile at 20;Inert atmosphere;
References:
Iannotta, Daniela;Castellucci, Nicola;Monari, Magda;Tomasini, Claudia [Tetrahedron Letters,2010,vol. 51,# 34,p. 4558 - 4559] Location in patent:experimental part
51077-16-8
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34592-47-7
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$5.00/5g
72744-67-3
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