6,7-Dihydro-2-phenyl-5H-pyrrolo[2,1-c]-1,2,4-triazolium chloride synthesis
- Product Name:6,7-Dihydro-2-phenyl-5H-pyrrolo[2,1-c]-1,2,4-triazolium chloride
- CAS Number:828914-68-7
- Molecular formula:C11H12N3.Cl
- Molecular Weight:221.69
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149-73-5
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828914-68-7
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Yield: 72%
Reaction Conditions:
Stage #1:2-pyrrolidinon;dimethyl sulfate in acetonitrile at 80; for 17 h;
Stage #2:phenylhydrazine in acetonitrile at 80; for 4 h;
Stage #3:trimethyl orthoformateFurther stages;
References:
Kena-diba, Anastasie;Noll, Claudia;Richter, Michael;Gieseler, Marc Timo;Kalesse, Markus [Angewandte Chemie - International Edition,2010,vol. 49,# 45,p. 8367 - 8369] Location in patent:supporting information; experimental part
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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149-73-5
512 suppliers
$12.00/5g
828914-68-7
41 suppliers
$70.00/100mg