N'-(2-Methoxybenzyl)-N,N-dimethylpropane-1,3-diamine synthesis
- Product Name:N'-(2-Methoxybenzyl)-N,N-dimethylpropane-1,3-diamine
- CAS Number:893595-46-5
- Molecular formula:C13H22N2O
- Molecular Weight:222.33
109-55-7
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893595-46-5
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Yield:-
Reaction Conditions:
Stage #1: 1-amino-3-(dimethylamino)propane;ortho-anisaldehyde in methanol; for 24 h;Reflux;Inert atmosphere;
Stage #2: with sodium tetrahydroborate in methanol at 20 - 50;Inert atmosphere;
References:
Song, Shaodi;Zhang, Xingyu;Ma, Haiyan;Yang, Yang [Dalton Transactions,2012,vol. 41,# 11,p. 3266 - 3277] Location in patent:experimental part