Alanine, 3-(benzyloxy)-N-carboxy-, di-tert-butyl ester (7CI) synthesis
- Product Name:Alanine, 3-(benzyloxy)-N-carboxy-, di-tert-butyl ester (7CI)
- CAS Number:95319-02-1
- Molecular formula:C19H29NO5
- Molecular Weight:351.44
Yield:95319-02-1 97%
Reaction Conditions:
Stage #1: tert-Butyl 2,2,2-trichloroacetimidate;BOC-O-benzyl-L-serinewith boron trifluoride diethyl etherate in dichloromethane;cyclohexane at 20; for 1 h;
Stage #2: with sodium hydrogencarbonate for 0.0833333 h;
References:
Xu, Youwen;Cankaya, Aylin Sibel;Hoque, Ruma;Lee, So Jeong;Shea, Colleen;Kersting, Lena;Schueller, Michael;Fowler, Joanna S.;Szalda, David;Alexoff, David;Riehl, Barbara;Gleede, Tassilo;Ferrieri, Richard A.;Qu, Wenchao [Chemistry - A European Journal,2018,vol. 24,# 26,p. 6848 - 6853] Location in patent:supporting information
24424-99-5
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$13.50/25G
23680-31-1
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$7.00/5g
95319-02-1
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![methyl (2S)-2-[(2-methylpropan-2-yl)oxycarbonylamino]-3-phenylmethoxypropanoate](/CAS/20180601/GIF/80963-10-6.gif)
23680-31-1
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$7.00/5g
95319-02-1
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