Adenine synthesis
- Product Name:Adenine
- CAS Number:73-24-5
- Molecular formula:C5H5N5
- Molecular Weight:135.13
A novel method for synthesizing adenine, comprising the steps of:
(1) firstly dispersing acetyl hypoxanthine in 1,2- dichloroethane, and then adding it to the reactor, slowly putting in anhydrous pyridine and triethylamine, stirring to raise th
Yield:73-24-5 81.8%
Reaction Conditions:
at 140 - 150; for 4 h;
Steps:
1
10 mL of formamide and 90 g of 4,5,6-triaminopyrimidine (Formula 6) were added to a 1000 mL reaction flask and heated to 140 to 150 ° C for 4 hours. The reaction was completed and cooled to a temperature of 25 to 15 ° C Crystallization, filtration, formamide rinsing, water elution, gray adipate crude, refined with water, activated carbon decolorization after 79.5g white crystalline powder adenine (Formula 1), yield 81.8%, HPLC 99.9%.
References:
CN106749043,2017,A Location in patent:Paragraph 0023
5667-20-9
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