AKOS BBS-00000713 synthesis
- Product Name:AKOS BBS-00000713
- CAS Number:63546-19-0
- Molecular formula:C10H11NO3
- Molecular Weight:193.2
108-24-7
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Yield:63546-19-0 91%
Reaction Conditions:
at 20; for 3 h;
Steps:
6.1
Example 6: Preparation of 2-[[4-(3-methoxylpropoxy)-3-methylipyridin-2-yl]methylsulfinyl]-6,7-dihydro-1H-[1,4]dioxino[2,3-f]benzimidazole(Compound 6) Step 1: Preparation of 6-acetylamino-2,3-dihydrobenzo[b][1,4]dioxane [Show Image] 6-amino-2,3-dihydrobenzo[b][1,4]dioxane (9 g, 60 mmol) and acetic anhydride (150 mL) were stirred at room temperature for 3 h, added to ice, extracted with dichloromethane (300 mL). The organic layer was dried, filtered, concentrated under vacuum to obtain a product (10.6 g, 91 %).
References:
EP2532665,2012,A1 Location in patent:Page/Page column 29
37866-47-0
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63546-19-0
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64-19-7
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75-36-5
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$17.92/100G
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197 suppliers
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63546-19-0
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