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21344-73-0

ALLYL-(4-PHENYL-THIAZOL-2-YL)-AMINE synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: potassium tert-butylate / tetrahydrofuran / 3 h / Inert atmosphere; Reflux
1.2: 16 h / 0 - 20 °C / Inert atmosphere
2.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride / 1,2-dichloro-ethane / 24 h / 80 °C

References:

Hassell-Hart, Storm;Speranzini, Elisa;Srikwanjai, Sirihathai;Hossack, Euan;Roe, S. Mark;Fearon, Daren;Akinbosede, Daniel;Hare, Stephen;Spencer, John [Organic Letters,2022,vol. 24,# 43,p. 7924 - 7927]