(BIS-TERT-BUTOXYCARBONYLMETHYL-AMINO)-ACETIC ACID synthesis
- Product Name:(BIS-TERT-BUTOXYCARBONYLMETHYL-AMINO)-ACETIC ACID
- CAS Number:171557-31-6
- Molecular formula:C14H25NO6
- Molecular Weight:303.35
![Glycine, N,N-bis[2-(1,1-dimethylethoxy)-2-oxoethyl]-, phenylmethyl ester](/CAS/20210305/GIF/171557-57-6.gif)
171557-57-6
171557-31-6
The compound (CAS: 171557-57-6, 477 mg, 1.17 mmol) was used as starting material, and the same synthesis method as compound 9 was used to obtain the target product N,N-di-BTBOC methylglycine (12, 335 mg, 97% yield), which was a light yellow oily product.
171557-57-6
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171557-31-6
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Yield:171557-31-6 97%
Reaction Conditions:
with palladium 10% on activated carbon;hydrogen in methanol at 20; for 2 h;
Steps:
Synthesis of 12
Compound 11 (477 mg, 1.17 mmol) was used as a starting material. By the same synthetic procedure as that for 9, 12 (335 mg, 97%) was obtained as a pale yellow oil.
References:
Takahira, Ikuko;Fuchida, Hirokazu;Tabata, Shigekazu;Shindo, Naoya;Uchinomiya, Shohei;Hamachi, Itaru;Ojida, Akio [Bioorganic and Medicinal Chemistry Letters,2014,vol. 24,# 13,p. 2855 - 2858] Location in patent:supporting information
49827-15-8
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171557-31-6
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5292-43-3
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171557-31-6
54 suppliers
$13.00/250mg