ChemicalBook CAS DataBase List coriandrin

coriandrin synthesis

8synthesis methods

Product Name:coriandrin
CAS Number:116408-80-1
Molecular formula:C13H10O4
Molecular Weight:230.22

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

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Yield:-

Steps:

Multi-step reaction with 6 steps
1: 100 percent / AcOK / 12 h / 120 °C
2: NBS, benzoyl peroxide / CCl₄ / 16 h / 120 °C
3: 87 percent / PhCH₂Pd(PPh₃)2Cl / hexamethylphosphoric acid triamide / 6 h / 65 °C
4: 75 percent / LiOH / methanol; tetrahydrofuran; H₂O / 40 h / 70 °C
5: 69 percent / Na₂CO₃, Pd(CH₃CN)2Cl₂ / tetrahydrofuran / 4 h / Ambient temperature
6: 89 percent / DEAD, Ph₃P / 6 h / Ambient temperature

References:

Kraus, George A.;Ridgeway, James [Journal of Organic Chemistry,1994,vol. 59,# 17,p. 4735 - 4737]

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References

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References

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References

67-56-1 Synthesis

67-56-1
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References

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