DI-N-AMYL SULFOXIDE synthesis
- Product Name:DI-N-AMYL SULFOXIDE
- CAS Number:4253-99-0
- Molecular formula:C10H22O2S
- Molecular Weight:206.35
Yield:-
Reaction Conditions:
with C42H30Fe2N6O6*C2H6O;urea hydrogen peroxide adduct in acetonitrile at 20; for 0.25 h;
Steps:
2.3. Catalytic sulfoxidation
General procedure: 0.2 mmol UHP as an oxidant was added slowly to a stirringsolution of 1 ml of CH3CN containing the complex [Fe2(salcyn)3],a substrate (0.2 mmol) and chlorobenzene (0.2 mmol) as an internalstandard. Stirring was continued for 15 min at room temperaturein a closed system. The reaction progress was monitored by GC. Assignments of the products were made by comparison with authentic samples.
References:
Akbari, Ali;Amini, Mojtaba;Bagherzadeh, Mojtaba;Ellern, Arkady;Mesbahi, Elnaz;Woo, L. Keith [Polyhedron,2020,vol. 183]
1986-90-9
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