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ChemicalBook CAS DataBase List Dichloroacetyl fluoride
359-31-9

Dichloroacetyl fluoride synthesis

6synthesis methods
-

Yield:661-75-6 74%

Reaction Conditions:

Stage #1: methoxyfluranewith potassium hydroxideHeating;Dehydrofluorination;
Stage #2: with chlorine at -40;Chlorination;
Stage #3: with antimonypentachloride at 40; for 0.833333 h;Fluorination;Decomposition;

References:

Ramig, Keith;Kudzma, Linas V.;Lessor, Ralph A.;Rozov, Leonid A. [Journal of Fluorine Chemistry,1999,vol. 94,# 1,p. 1 - 5]