ChemicalBook CAS DataBase List DIPHENAMID

DIPHENAMID synthesis

6synthesis methods

Product Name:DIPHENAMID
CAS Number:957-51-7
Molecular formula:C16H17NO
Molecular Weight:239.31

The commercial production of diphenamid involves a multi-step process. It begins with the reaction of diphenylacetic acid with thionyl chloride to form diphenylacetyl chloride, which is then reacted with dimethylamine in an organic solvent, such as toluene, under controlled temperature to produce the amide linkage. The reaction is carefully monitored to optimise yield and minimise byproducts.

Benzeneethanimidoyl chloride, N-hydroxy-α-phenyl-

4467-90-7
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inquiry

957-51-7
78 suppliers
$53.50/100mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1: sodium carbonate / H₂O / 1.5 h / 55 - 60 °C / nonionic tenside
2: 92 percent / 1.) aq. NaNO₂, sodium laurylosulphonate, 2.) aq. H₂SO₄ / 2.) 4 h

References:

Eckstein, Z.;Jelenski, P.;Kowal, J.;Rusek, D. [Synthetic Communications,1982,vol. 12,# 3,p. 201 - 208]

90-99-3 Synthesis

90-99-3
278 suppliers
$9.00/5g

479486-96-9
5 suppliers
inquiry

957-51-7
78 suppliers
$53.50/100mg

References

117-34-0 Synthesis

117-34-0
287 suppliers
$6.00/10g

124-40-3
517 suppliers
$18.00/100ml

957-51-7
78 suppliers
$53.50/100mg

References

591-50-4 Synthesis

591-50-4
467 suppliers
$10.00/1g

127-19-5 Synthesis

127-19-5
835 suppliers
$5.00/25g

18925-69-4
49 suppliers
$15.00/5mg

957-51-7
78 suppliers
$53.50/100mg

References

1871-76-7
163 suppliers
$12.00/1g

124-40-3
517 suppliers
$18.00/100ml

957-51-7
78 suppliers
$53.50/100mg

References

DIPHENAMID Related Search:

Loperamide hydrochloride Loperamide Oxanilide N,N-Dimethylacetamide

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