ErtapeneM IMpurity DIPP synthesis
- Product Name:ErtapeneM IMpurity DIPP
- CAS Number:220031-86-7
- Molecular formula:C18H27N2O6PS
- Molecular Weight:430.46
117286-92-7
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220031-86-7
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: 56 percent / (i-Pr)2NEt / CH2Cl2 / 0.25 h / -15 °C
2.1: pyridine / CH2Cl2 / 0.5 h / -20 °C
3.1: Na2S*3H2O / CH2Cl2; H2O / 0.03 h
3.2: 5 g / CH2Cl2; H2O / 2.08 h / 3 - 25 °C
4.1: acetic acid / 20 - 23 °C
References:
Brands, Karel M J;Jobson, Ronald B;Conrad, Karen M;Williams, J Michael;Pipik, Brenda;Cameron, Mark;Davies, Antony J;Houghton, Peter G;Ashwood, Michael S;Cottrell, Ian F;Reamer, Robert A;Kennedy, Derek J;Dolling, Ulf-H;Reider, Paul J [Journal of Organic Chemistry,2002,vol. 67,# 14,p. 4771 - 4776]
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