FaMciclovir iMpurity 7 synthesis
- Product Name:FaMciclovir iMpurity 7
- CAS Number:127205-22-5
- Molecular formula:C10H15N5O3
- Molecular Weight:253.26
17495-12-4
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Yield:-
Steps:
Multi-step reaction with 7 steps
1.1: 93 percent / 1-methyl-pyrrolidin-2-one / 1 h / 150 °C
2.1: 90 percent / 1-methyl-pyrrolidin-2-one / 2 h / 120 °C
3.1: HCOONH4 / Pd/C / methanol / 4 h / Heating
3.2: 71 percent / NH4OH / 1 h / Heating
4.1: 46 percent / 1-methyl-pyrrolidin-2-one / 4 h / 150 °C
5.1: 99 percent / 1-methyl-pyrrolidin-2-one / 20 h / 120 °C
6.1: HCOONH4 / Pd/C / methanol / 4 h / Heating
7.1: 132 mg / aq. NaOH / 0.5 h / Heating
References:
Kalayanov, Genadiy;Jaksa, Suzana;Scarcia, Tommaso;Kobe, Joze [Synthesis,2004,# 12,p. 2026 - 2034]
![Acetamide, N-[6,7-dihydro-6-oxo-7-(phenylmethyl)-1H-purin-2-yl]-](/CAS/20210305/GIF/17495-10-2.gif)
17495-10-2
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![Acetamide, N-[6,9-dihydro-6-oxo-9-(phenylmethyl)-1H-purin-2-yl]-](/CAS/20210305/GIF/17495-11-3.gif)
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127205-22-5
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19962-37-9
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$9.00/250mg
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73-40-5
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$5.00/5g
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