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ChemicalBook CAS DataBase List Phenylundecanoic acid
3343-24-6

Phenylundecanoic acid synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 76 percent / tin(IV) chloride / CH2Cl2 / 1.5 h / Ambient temperature
2: 91 percent / 95percent hydrazine hydrate, potassium hydroxide / ethane-1,2-diol / 4.5 h / 60 °C / Heating
3: 85 percent / Raney nickel-aluminium alloy / aq. NaOH / 3 h / 90 - 120 °C

References:

Jefferson, Alan;Sargent, Melvyn V.;Wangchareontrakul, Sirichai [Australian Journal of Chemistry,1988,vol. 41,# 1,p. 19 - 25]