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1078-74-6

Thiirane, decyl- synthesis

2synthesis methods
55334-42-4 Synthesis
1,2-Dibromododecane

55334-42-4
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) sodium sulfide nonahydrate / 1.) Aliquat 336 / 1.) water, 2.) 70 deg C, 1 h
2: 1.) HBF4*Et2O, 2.) 1,2-epoxydodecane / 1.) Et2O, CH2Cl2, 0-5 deg C, 2.) r.t.

References:

Barbero, Margherita;Degani, Iacopo;Dughera, Stefano;Fochi, Rita;Piscopo, Laura [Journal of the Chemical Society. Perkin transactions I,1996,# 3,p. 289 - 294]