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ChemicalBook CAS DataBase List Triethanolamine 2,4-dichlorophenoxyacetate
2569-01-9

Triethanolamine 2,4-dichlorophenoxyacetate synthesis

1synthesis methods
Commercial production of 2,4 D trolamine follows the same industrial pathway used for other amine salts of 2,4 D, a long established phenoxyacetic acid herbicide. Manufacturers first produce technical grade 2,4 D acid, then neutralise it with triethanolamine (trolamine) under controlled aqueous conditions to form the highly water soluble trolamine salt.
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Yield:2569-01-9 96.2%

Reaction Conditions:

in ethanol;

References:

Voronkov, M. G.;Semenova, N. V.;Kazimirovskaya, V. B.;Kholdeeva, L. N.;Moskvitina, L. T.;et al. [Pharmaceutical Chemistry Journal,1986,vol. 20,# 8,p. 555 - 558][Khimiko-Farmatsevticheskii Zhurnal,1986,vol. 20,# 8,p. 952 - 956]

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