Triisobutylaluminum synthesis
1synthesis methods
- Product Name:Triisobutylaluminum
- CAS Number:100-99-2
- Molecular formula:C12H27Al
- Molecular Weight:198.32
Triisobutylaluminum can be prepared by the reaction of activated aluminum with hydrogen and isobutylene at elevated temperature and pressure. The usual procedure for carrying out the reaction has been to charge activated aluminum, customarily as a slurry in the previously prepared product when available, sufficient isobutylene for the conversion of a substantial amount of the aluminum, and finally, sufficient hydrogen pressure, incrementally to maintain an acceptable reaction rate.
115-11-7
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$45.00/25 g
100-99-2
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$81.10/100ml
Yield:-
Reaction Conditions:
with hydrogen;aluminium
References:
Ziegler;Lehmkuhl [Angewandte Chemie,1955,vol. 67,p. 424] Ziegler;Gellert US2835689, 1955