Vat Red 32 synthesis
- Product Name:Vat Red 32
- CAS Number:2379-77-3
- Molecular formula:C36H16Cl2N2O4
- Molecular Weight:611.43
![2-(4-chlorophenyl)-1H-benzo[de]isoquinoline-1,3(2H)-dione](/CAS/20180711/GIF/6915-00-0.gif)
6915-00-0
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2379-77-3
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Yield:2379-77-3 96%
Reaction Conditions:
with 1-methyl-1H-imidazole;DBN;sodium n-propoxide;1,8-diazabicyclo[5.4.0]undec-7-ene at 140 - 160; for 6 h;
Steps:
4 Example 4
Dehydrated 90g N-methylimidazole and 10g were added to a 500ml four-necked flask DBU and 200g BDN,12 g of N-(4-chlorophenyl)naphthalimide and 0.36 g of sodium n-propoxide were added while stirring.After heating at 160 ° C and reacting at 140 ° C for 6 hours, cooling, the reaction system was transferred to a rotary evaporator.Distilling under reduced pressure to recover the solvent;The solid product was washed sequentially with water and DMF.Get the red product,The yield was 96%.
References:
CN109535767,2019,A Location in patent:Paragraph 0033; 0034
![Anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,10-dione, 2,9-bis(4-chlorophenyl)-2,3,8,9-tetrahydro-3,8-dihydroxy- (9CI)](/CAS/20210305/GIF/150106-94-8.gif)
150106-94-8
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2379-77-3
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